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Beilstein J. Org. Chem. 2014, 10, 2122–2130, doi:10.3762/bjoc.10.219
Graphical Abstract
Figure 1: Previously reported indeno[1,2-b]fluorenes and related indeno[1,2-b]fluorene-6,12-diones.
Scheme 1: Transannular cyclization route to diethynyl-IF-diones 8.
Scheme 2: Suzuki/Friedel-Crafts route to diethynyl-IF-diones 8.
Figure 2: UV–vis spectrum (left) and cyclic voltammogram (right) of dione 8c.
Figure 3: Kohn–Sham HOMO (left) and LUMO (right) plots of 8a.
Figure 4: Views perpendicular to the average plane of the π stack. 1st row left to right – 8a, 8b, 8c; 2nd ro...
Figure 5: Schematic of the parameters used for comparing X-ray crystal structures, view is parallel to the mo...